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By Hermans, Sophie; Bocarme, Thierry Visart De

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41. N. Millot, C. C. Santini, F. Lefebvre and J. M. Basset, C. R. , 2004, 7, 725–736. 42. M. E. Bartram, T. A. Michalske and J. W. , J. Phys. , 1991, 95, 4453–4463. 43. E. Grinenval, X. Rozanska, A. Baudouin, E. Berrier, F. Delbecq, P. Sautet, J. M. Basset and F. Lefebvre, J. Phys. Chem. C, 2010, 114, 19024–19034. 44. B. C. Gerstein, M. -J. Hwang, Anal. Chim. Acta, 1993, 283, 1059–1079. ´ Claude Bernard-Lyon 1, 45. R. P. Saint-Arroman, PhD Thesis, Universite Lyon, 2002. 46. -M. Basset, A. Baudouin, F.

The dimensions are in Å. Adapted from ref. 56. 2). CO ligands in Rh(CO)2(acac) and those in the supported Rh(CO)2 show different n CO frequencies; IR data characterizing Rh(CO)2(acac) in a THF solution gives two sharp n CO bands (FWHMo5 cmÀ1) at 2010 cmÀ1 (symmetric band) and 2081 cmÀ1 (antisymmetric band) because of C2v symmetry of this complex. 99 in water at 298 K), rhodium atoms in chemisorbed rhodium complexes are more electron deficient. Thus, rhodium atoms in the chemisorbed complexes back-donate less electron density to an antibonding orbital of CO, leading to a blue shift of CO stretching band.

Le Roux, R. M. Gauvin, F. Lefebvre, J. -M. Basset, J. Organomet. , 2008, 693, 1733–1737. 54. X. Solans-Monfort, J. S. Filhol, C. Coperet and O. Eisenstein, New J. , 2006, 30, 842–850. 55. N. Merle, J. Trebosc, A. Baudouin, I. D. Rosal, L. Maron, K. Szeto, M. Genelot, A. Mortreux, M. Taoufik, L. Delevoye and R. M. Gauvin, J. Am. Chem. , 2012, 134, 9263–9275. 56. B. Rhers, E. A. Quadrelli, A. Baudouin, M. Taoufik, C. Coperet, F. -M. Basset, B. Fenet, A. Sinha and R. R. Schrock, J. Organomet. , 2006, 691, 5448–5455.

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